Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU
Yıl: 2022 Cilt: 10 Sayı: 4 Sayfa Aralığı: 965 - 975 Metin Dili: Türkçe DOI: 10.36306/konjes.1148331 İndeks Tarihi: 16-12-2022
Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU
Öz: Bu çalışmada, Ni-FeNi3-Fe3O4 metalik nanoalaşımlar hidrotermal yöntem kullanılarak 180 °C’de 2 saatte başarılı bir şekilde sentezlenmiştir. Sentezi gerçekleştirilen metalik nanoalaşımların yapısal ve morfolojik özellikleri X-ışını Kırınımı (XRD), Fourier Dönüşümlü Infrared Spektrofotometresi (FTIR) ve Taramalı Elektron Mikroskobu (SEM) kullanılarak karakterize edilmiştir. X-ışını Kırınım metodu sonucu elde edilen kırınım desenleri incelendiğinde yüksek şiddetli piklerin kübik kristal yapıdaki FeNi3 ve metalik Ni’e ait olduğu belirlenmiştir. Daha düşük şiddette elde edilen piklerin ise Fe3O4 yapısına ait olduğu gösterilmiştir. FTIR analizi sonucu 455,2 ve 570,9 cm-1’de elde edilen piklerin sırasıyla Fe-Ni ve Fe-O bağlarına ait karakteristik pik olduğu gösterilmiştir. SEM-EDS analizlerinden ise sentezlenen metalik nanoalaşımlar ortalama yarıçapı 3,51 μm olan küresel parçacıkların metalik Ni fazı olduğu ve yüzeylerin bir miktar FeNi3 nanoparçacıkları ile kaplandığı görülmüştür. Ortalama yarıçapı 63,33 nm olan düzensiz şekilli nanoparçacıkların ise Fe3O4 ile birlikte FeNi3 yapısında olduğu belirlenmiştir.
Anahtar Kelime: Synthesis and Characterization of Ni-FeNi3-Fe3O4 Metallic Nanoalloys by Hydrothermal Method
Öz: In this study, Ni-FeNi3-Fe3O4 metallic nanoalloys were successfully synthesized using the hydrothermal method at 180 °C for 2 hours. The structural and morphological properties of the synthesized metallic nanoalloys were characterized using X-ray diffraction (XRD), Fourier Transform Infrared Spectrophotometer (FTIR) and Scanning Electron Microscopy (SEM). When the diffraction patterns obtained from XRD analysis, it was determined that the high intensity peaks belonged to FeNi3 with cubic crystal structure and metallic Ni. It has been shown that the peaks obtained at lower intensity belong to the Fe3O4 structure. As a result of the FTIR analysis, the peaks obtained at 455.2 and 570.9 cm-1 were shown to be characteristic peaks of Fe-Ni and Fe-O bonds, respectively. SEM-EDS images showed that the synthesized metallic nanoalloys spherical particles with an average radius of 3.51 μm were the metallic Ni phase and the surfaces were covered with some FeNi3. It was determined that irregular shaped nanoparticles with an average radius of 63.33 nm were in FeNi3 structure together with Fe3O4.
Anahtar Kelime: Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık
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| APA | ATAS M, ALTINTAS YILDIRIM O (2022). Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. , 965 - 975. 10.36306/konjes.1148331 |
| Chicago | ATAS Mehmet Sahin,ALTINTAS YILDIRIM OZLEM Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. (2022): 965 - 975. 10.36306/konjes.1148331 |
| MLA | ATAS Mehmet Sahin,ALTINTAS YILDIRIM OZLEM Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. , 2022, ss.965 - 975. 10.36306/konjes.1148331 |
| AMA | ATAS M,ALTINTAS YILDIRIM O Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. . 2022; 965 - 975. 10.36306/konjes.1148331 |
| Vancouver | ATAS M,ALTINTAS YILDIRIM O Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. . 2022; 965 - 975. 10.36306/konjes.1148331 |
| IEEE | ATAS M,ALTINTAS YILDIRIM O "Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU." , ss.965 - 975, 2022. 10.36306/konjes.1148331 |
| ISNAD | ATAS, Mehmet Sahin - ALTINTAS YILDIRIM, OZLEM. "Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU". (2022), 965-975. https://doi.org/10.36306/konjes.1148331 |
| APA | ATAS M, ALTINTAS YILDIRIM O (2022). Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. Konya mühendislik bilimleri dergisi (Online), 10(4), 965 - 975. 10.36306/konjes.1148331 |
| Chicago | ATAS Mehmet Sahin,ALTINTAS YILDIRIM OZLEM Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. Konya mühendislik bilimleri dergisi (Online) 10, no.4 (2022): 965 - 975. 10.36306/konjes.1148331 |
| MLA | ATAS Mehmet Sahin,ALTINTAS YILDIRIM OZLEM Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. Konya mühendislik bilimleri dergisi (Online), vol.10, no.4, 2022, ss.965 - 975. 10.36306/konjes.1148331 |
| AMA | ATAS M,ALTINTAS YILDIRIM O Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. Konya mühendislik bilimleri dergisi (Online). 2022; 10(4): 965 - 975. 10.36306/konjes.1148331 |
| Vancouver | ATAS M,ALTINTAS YILDIRIM O Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU. Konya mühendislik bilimleri dergisi (Online). 2022; 10(4): 965 - 975. 10.36306/konjes.1148331 |
| IEEE | ATAS M,ALTINTAS YILDIRIM O "Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU." Konya mühendislik bilimleri dergisi (Online), 10, ss.965 - 975, 2022. 10.36306/konjes.1148331 |
| ISNAD | ATAS, Mehmet Sahin - ALTINTAS YILDIRIM, OZLEM. "Ni-FeNi3-Fe3O4 METALİK NANOALAŞIMLARIN HİDROTERMAL YÖNTEMLE SENTEZİ VE KARAKTERİZASYONU". Konya mühendislik bilimleri dergisi (Online) 10/4 (2022), 965-975. https://doi.org/10.36306/konjes.1148331 |
