Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi

Demirci, Sevilay; BAYTAR, ORHAN; Beştaş, Hatice; İZGİ, Mehmet Sait; ONAT, Erhan; ŞAHİN, Ömer

doi:10.30728/boron.1179156

Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi

Hatice BEŞTAŞ, (Siirt Üniversitesi, Mühendislik Fakültesi, Kimya Mühendisliği Bölümü, Siirt, Türkiye)

Erhan ONAT, (Siirt Üniversitesi, Mühendislik Fakültesi, Kimya Mühendisliği Bölümü, Siirt, Türkiye)

Ömer ŞAHİN, (İstanbul Teknik Üniversitesi, Mühendislik Fakültesi, Kimya Mühendisliği Bölümü, İstanbul, Türkiye)

Sevilay DEMİRCİ, (Kafkas Üniversitesi, Mühendislik Mimarlık Fakültesi, Kimya Mühendisliği Bölümü, Kars, Türkiye)

Orhan BAYTAR, (Siirt Üniversitesi, Mühendislik Fakültesi, Kimya Mühendisliği Bölümü, Siirt, Türkiye)

Mehmet Sait İZGİ (Siirt Üniversitesi, Mühendislik Fakültesi, Kimya Mühendisliği Bölümü, Siirt, Türkiye)

BOR DERGİSİ

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Yıl: 2023 Cilt: 8 Sayı: 2 Sayfa Aralığı: 59 - 65 Metin Dili: Türkçe DOI: 10.30728/boron.1179156 İndeks Tarihi: 12-09-2023

Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi

Öz:

Bu çalışmada ilk kez kahve çekirdeği atığından (kahve telvesinden) elde edilen aktif karbon kullanılarak CuMoB@AC ilk kez katalizörü sentezlendi. Burada en iyi katalitik performanslarını belirlemek amacıyla; Cu:Mo oranı, Metal/AC oranı, optimum NaOH oranı, katalizör miktarı, en uygun NH 3 BH 3 oranı ve farklı sıcaklıklarda yapılan deneyler sonucunda da reaksiyon kinetiği çıkarılarak reaksiyonun derecesinin n. dereceden (0.9) olduğu ve aktivasyon enerjisinin de 34,89 kJ/mol olduğu belirlendi. Aynı zamanda katalizörümüz karakterizasyonu belirlemek için SEM-EDS, XRD ileri analitiksel yöntemler kullanılarak belirlenmiştir.

Anahtar Kelime: Amonyak boran CuMoB Hidrojen Hidroliz

Investigation of a cheap and useful activated carbon supported catalyst in ammonia boron hydrolysis

Öz:

In this study, CuMoB@AC catalyst was synthesized for the first time by using activated carbon obtained from coffee bean waste (coffee grounds). In order to determine the best catalytic performances; Cu:Mo ratio, Metal/AC ratio, optimum NaOH ratio, catalyst amount, optimum NH3BH3 ratio and reaction kinetics were determined as a result of experiments performed at different temperatures. It was determined that the degree of the reaction was n. degree (0.9) and the activation energy was 34.89 kJ/mol. At the same time, our catalyst was determined using SEM-EDS, XRD advanced analytical methods to determine the characterization.

Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	Beştaş H, ONAT E, ŞAHİN Ö, Demirci S, BAYTAR O, İZGİ M (2023). Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. , 59 - 65. 10.30728/boron.1179156
Chicago	Beştaş Hatice,ONAT Erhan,ŞAHİN Ömer,Demirci Sevilay,BAYTAR ORHAN,İZGİ Mehmet Sait Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. (2023): 59 - 65. 10.30728/boron.1179156
MLA	Beştaş Hatice,ONAT Erhan,ŞAHİN Ömer,Demirci Sevilay,BAYTAR ORHAN,İZGİ Mehmet Sait Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. , 2023, ss.59 - 65. 10.30728/boron.1179156
AMA	Beştaş H,ONAT E,ŞAHİN Ö,Demirci S,BAYTAR O,İZGİ M Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. . 2023; 59 - 65. 10.30728/boron.1179156
Vancouver	Beştaş H,ONAT E,ŞAHİN Ö,Demirci S,BAYTAR O,İZGİ M Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. . 2023; 59 - 65. 10.30728/boron.1179156
IEEE	Beştaş H,ONAT E,ŞAHİN Ö,Demirci S,BAYTAR O,İZGİ M "Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi." , ss.59 - 65, 2023. 10.30728/boron.1179156
ISNAD	Beştaş, Hatice vd. "Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi". (2023), 59-65. https://doi.org/10.30728/boron.1179156

APA	Beştaş H, ONAT E, ŞAHİN Ö, Demirci S, BAYTAR O, İZGİ M (2023). Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. BOR DERGİSİ, 8(2), 59 - 65. 10.30728/boron.1179156
Chicago	Beştaş Hatice,ONAT Erhan,ŞAHİN Ömer,Demirci Sevilay,BAYTAR ORHAN,İZGİ Mehmet Sait Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. BOR DERGİSİ 8, no.2 (2023): 59 - 65. 10.30728/boron.1179156
MLA	Beştaş Hatice,ONAT Erhan,ŞAHİN Ömer,Demirci Sevilay,BAYTAR ORHAN,İZGİ Mehmet Sait Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. BOR DERGİSİ, vol.8, no.2, 2023, ss.59 - 65. 10.30728/boron.1179156
AMA	Beştaş H,ONAT E,ŞAHİN Ö,Demirci S,BAYTAR O,İZGİ M Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. BOR DERGİSİ. 2023; 8(2): 59 - 65. 10.30728/boron.1179156
Vancouver	Beştaş H,ONAT E,ŞAHİN Ö,Demirci S,BAYTAR O,İZGİ M Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi. BOR DERGİSİ. 2023; 8(2): 59 - 65. 10.30728/boron.1179156
IEEE	Beştaş H,ONAT E,ŞAHİN Ö,Demirci S,BAYTAR O,İZGİ M "Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi." BOR DERGİSİ, 8, ss.59 - 65, 2023. 10.30728/boron.1179156
ISNAD	Beştaş, Hatice vd. "Aktif karbon destekli ucuz ve kullanışlı katalizörün amonyak bor hidrolizinde incelenmesi". BOR DERGİSİ 8/2 (2023), 59-65. https://doi.org/10.30728/boron.1179156