Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography
Yıl: 2023 Cilt: 27 Sayı: 5 Sayfa Aralığı: 1002 - 1007 Metin Dili: İngilizce DOI: 10.16984/saufenbilder.1265507 İndeks Tarihi: 26-10-2023
Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography
Öz: In this study, a high performance liquid chromatography-ultraviolet detection method was introduced for the detection of cymoxanil. The experimental parameters of the procedure were thoroughly evaluated. Cymoxanil was eluted by ammonium formate buffer (50.0 mM, pH 4.0):acetonitrile (55:45 v/v) as mobile phase. Under the optimal conditions, the limits of detection and quantification (LOD and LOQ) were found as 7.4 – 24.8 µg kg-1, which allows trace determination of pesticides in food samples. Proposed method was then implemented for the determination of selected fungicide in potato flour samples with acceptable % recoveries in the range of 81.4–112.9%, while the values of relative standard deviation (RSD) were below 10% showing a satisfactory applicability for cymoxanil in such complex real samples matrix.
Anahtar Kelime: Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık
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APA | Unutkan" T (2023). Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. , 1002 - 1007. 10.16984/saufenbilder.1265507 |
Chicago | Unutkan" Tuğçe Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. (2023): 1002 - 1007. 10.16984/saufenbilder.1265507 |
MLA | Unutkan" Tuğçe Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. , 2023, ss.1002 - 1007. 10.16984/saufenbilder.1265507 |
AMA | Unutkan" T Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. . 2023; 1002 - 1007. 10.16984/saufenbilder.1265507 |
Vancouver | Unutkan" T Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. . 2023; 1002 - 1007. 10.16984/saufenbilder.1265507 |
IEEE | Unutkan" T "Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography." , ss.1002 - 1007, 2023. 10.16984/saufenbilder.1265507 |
ISNAD | Unutkan", Tuğçe. "Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography". (2023), 1002-1007. https://doi.org/10.16984/saufenbilder.1265507 |
APA | Unutkan" T (2023). Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 27(5), 1002 - 1007. 10.16984/saufenbilder.1265507 |
Chicago | Unutkan" Tuğçe Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi 27, no.5 (2023): 1002 - 1007. 10.16984/saufenbilder.1265507 |
MLA | Unutkan" Tuğçe Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi, vol.27, no.5, 2023, ss.1002 - 1007. 10.16984/saufenbilder.1265507 |
AMA | Unutkan" T Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi. 2023; 27(5): 1002 - 1007. 10.16984/saufenbilder.1265507 |
Vancouver | Unutkan" T Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi. 2023; 27(5): 1002 - 1007. 10.16984/saufenbilder.1265507 |
IEEE | Unutkan" T "Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography." Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 27, ss.1002 - 1007, 2023. 10.16984/saufenbilder.1265507 |
ISNAD | Unutkan", Tuğçe. "Development of an Analytical Method for the Determination of Cymoxanil in Potato Flour Samples by High Performance Liquid Chromatography". Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi 27/5 (2023), 1002-1007. https://doi.org/10.16984/saufenbilder.1265507 |