TY  - JOUR
TI  - Application of experimental design on determination of aluminum content in saline samples by adsorptive cathodic stripping voltammetry
AB  - Adsorptive cathodic stripping voltammetric determination of aluminum at ng mL -1 levels in salt samples based on the metal complexation with Calcon (1-(2-hydroxynaphthylazo)-2 naphthol-4-sulfonic acid) and the subsequent adsorptive deposition onto a hanging mercury drop electrode was studied. Central composite design was used as a design method. Several chemical and instrumental parameters (pH, ligand concentration, deposition time, deposition potential, and complexing time) were involved in the experimental design. Analytical parameters such as repeatability, linearity, and accuracy were also investigated and the detection limit was found as 0.32 ng mL -1 .
AU  - Ertaş, Fatma Nil
AU  - ÖZDEMİR, Durmuş
AU  - EROĞLU, Ahmet Emin
AU  - YILMAZ, Sinan
AU  - ÖZTÜRK, BETÜL
PY  - 2013
JO  - Turkish Journal of Chemistry
VL  - 37
IS  - 2
SN  - 1300-0527
SP  - 316
EP  - 324
DB  - TRDizin
UR  - http://search/yayin/detay/146205
ER  -