Supramolecular solvent microextraction of uranium at trace levels from water and soil samples

YILMAZ, Erkan; Soylak, Mustafa; Khan, Mansoor

Supramolecular solvent microextraction of uranium at trace levels from water and soil samples

Mansoor KHAN, (Erciyes Üniversitesi, Fen Edebiyat Fakültesi, Kimya Bölümü, Kayseri, Türkiye)

Erkan YILMAZ, (Erciyes Üniversitesi, Fen Edebiyat Fakültesi, Kimya Bölümü, Kayseri, Türkiye)

Mustafa SOYLAK (Erciyes Üniversitesi, Fen Edebiyat Fakültesi, Kimya Bölümü, Kayseri, Türkiye)

Turkish Journal of Chemistry

1 0

Yıl: 2017 Cilt: 41 Sayı: 1 Sayfa Aralığı: 61 - 69 Metin Dili: İngilizce İndeks Tarihi: 29-07-2022

Supramolecular solvent microextraction of uranium at trace levels from water and soil samples

Öz:

A supramolecular solvent microextraction procedure was established for the separation/preconcentration of uranium(VI) (U(VI)) prior to its determination by UV-Vis spectrophotometry. 1-(2-Pyridylazo)-2-naphthol (PAN) was used to form a red chelate (U-PAN) with U(VI) at pH 10. U-PAN was extracted by undecanol in tetrahydrofuran. All the parameters that affect extraction efficiency like solution pH, amount of ligand, type and volume of supramolecular solvent, sample volume, and diverse ion effect were optimized. The preconcentration factor was 17. The detection limit was 0.31 µg L −1 . The method was validated using GBW07424 (GSS-10 certified reference material). Microextraction was also applied to water and soil samples.

Anahtar Kelime:

Konular: Mühendislik, Kimya

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

1. Aydin, F. A.; Soylak, M. Talanta 2007, 72, 187-192.
2. Shah, F.; Soylak, M.; Kazi, T. G.; Afridi, H. I. J. Radioanal. Nucl. Chem. 2013, 296, 1239-1245.
3. Yousefi, S. R.; Ahmadi, S. J.; Shemirani, F.; Jamali, M. R.; Salavati-Niasari, M. Talanta 2009, 80, 212-217.
4. Ghasemi, J. B.; Zolfonoun, E. Talanta 2010, 80, 1191-1197.
5. Madrakian, T.; Afkhami, A.; Mousavi, A. Talanta 2007, 71, 610-614.
6. Suresh, A.; Patre, D. K.; Srinivasan, T. G.; Rao, P. R. V. Spectrochim. Acta 2002, 58A, 341-347.
7. Jamali, M. R.; Assadi, Y.; Shemirani, F.; Hosseini, M. R. M.; Kozani, R. R.; Masteri-Farahani, M.; Salavati-Niasari, M. Anal. Chim. Acta 2006, 579, 68-73.
8. Nivens, D. A.; Zhang, Y.; Angel, S. M. J. Photochem. Photobiol. A: Chem. 2002, 152, 167-173.
9. Lutfullah, M. N.; Alam, N. R.; Azmi, S. N. H. J. Hazard. Mater. 2008, 155, 261-268.
10. Hassan, E. M. J. Pharm. Biomed. Anal. 2002, 27, 771-777.
11. Ramakrishna, T.; Murthy, R. S. Talanta 1980, 27, 442-444.
12. Madrakian, T.; Afkhami, A.; Mousavi, A. Talanta 2007, 71, 610-614.
13. Das, S.; Kedari, C.; Tripathi, S. J. Radioanal. Nucl. Chem. 2010, 285, 675-681.
14. Shemirani, F.; Rahnama Kozani, R.; Reza Jamali, M.; Assadi, Y.; Mohammad Reza Milani, S. Sep. Sci. Technol. 2005, 40, 2527-2537.
15. Amin, A. S. Spectrosc. Lett. 2012, 45, 246-255.
16. Currah, J.; Beamish, F. Anal. Chem. 1947, 19, 609-612.
17. Ouadi, A.; Klimchuk, O.; Gaillard, C.; Billard, I. Green Chem. 2007, 9, 1160-1162.
18. Shamsipur, M.; Ghiasv, A. R.; Yamini, Y. Anal. Chem. 1999, 71, 4892-4895.
19. Ojeda, C. B.; Rojas, F. S. Anal. Bioanal. Chem. 2009, 394, 759-782.
20. Chandrasekaran, K.; Karunasagar, D.; Arunachalam, J. Anal. Methods 2011, 3, 2140-2147.
21. Jahromi, E. Z.; Bidari, A.; Assadi, Y.; Hosseini, M. R. M.; Jamali, M. R. Anal. Chim. Acta 2007, 585, 305-311.
22. Zang, X. H.; Wu, Q. H.; Zhang, M. Y.; Xi, G. H.; Wang, Z. Chin. J. Anal. Chem. 2009, 37, 161-168. 23. Karadas, C. Water Air Soil Pollut. 2014, 225, 1-9.
24. Hu, B.; He, M.; Chen, B.; Xia, L. Spectrochim. Acta 2013, 86B, 14-30.
25. Yilmaz, E.; Soylak, M. Talanta 2013, 116, 882-886.
26. Yilmaz, E.; Soylak, M. Talanta 2014, 126, 191-195.
27. Soylak, M.; Khan, M.; Yilmaz, E. Anal. Methods 2016, 8, 979-986.
28. Jafarv, S.; Shemirani, F. Anal. Methods 2011, 3, 1552-1559.
29. L´opez-Jim´enez, F. J.; Rubio, S.; P´erez-Bendito, D. Food Chem. 2010, 121, 763-769.
30. Garc´ıa-Fonseca, S.; Ballesteros-G´omez, A.; Rubio, S.; P´erez-Bendito, D. J. Chromatogr. 2010, 1217A, 2376-2382.
31. Shibata, S. Anal. Chim. Acta 1960, 22, 479-484.
32. Gill, H.; Rolf, R.; Armstrong, G. Anal. Chem. 1958, 30, 1788-1792.
33. Khayatian, G.; Hassanpoor, S.; Azar, A. R.; Mohebbi, S. J. Braz. Chem. Soc. 2013, 24, 1808-1817.
34. Jalbani, N.; Soylak, M. J. Ind. Eng. Chem. 2015, 29, 48-51.
35. Ghaedi, M.; Ahmadi, F.; Tavakoli, Z.; Montazerozohori, M.; Khanmohammadi, A.; Soylak, M. J. Hazard. Mater. 2008, 152, 1248-1255.
36. Dasbasi, T.; Sa¸cmacı, S¸.; Ulgen, A.; Kartal, S¸. ¨ J. Ind. Eng. Chem. 2015, 28, 316-321.
37. Soylak, M.; Yilmaz, E. Desalination 2011, 275, 297-301.
38. Rastegarzadeh, S.; Pourreza, N.; Larki, A. J. Ind. Eng. Chem. 2015, 24, 297-301.
39. Al-Othman, Z. A.; Habila, M.; Yilmaz, E.; Soylak, M. J. AOAC Int. 2013, 96, 1425-1429.
40. Zhao, S. L.; Chen, F. S.; Zhang, J.; Ren, S. B.; Liang, H. D.; Li, S. S. J. Ind. Eng. Chem. 2015, 27, 362-367.
41. Kandhro, G. A., Kazi, T. G.; Soylak, M. Atom. Spectrosc. 2014, 35, 270-274.
42. Unsal, Y. E.; Tuzen, M.; Soylak, M. Turk. J. Chem. 2014, 38, 173-181.
43. Ozcan, S. G.; Satiroglu, N.; Soylak, M. Food Chem. Toxicol. 2010, 48, 2401-2406.
44. Bazmegan-shamili, A.; Haji Shabani, A. M.; Dadfarnia, S. Turk. J. Chem. 2015, 39, 1059-1068.
45. Tuzen, M.; Sari, A.; Mendil, D.; Soylak, M. J. Hazard. Mater. 2009, 169, 263-270.
46. Jalbani, N.; Soylak, M. J. Radioanal. Nucl. Chem. 2014, 301, 263-268.
47. Liu, Y.; Cao, X.; Le, Z.; Luo, M.; Xu, W.; Huang, G. J. Braz. Chem. Soc. 2010, 21, 533-540.

APA	Khan M, YILMAZ E, Soylak M (2017). Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. , 61 - 69.
Chicago	Khan Mansoor,YILMAZ Erkan,Soylak Mustafa Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. (2017): 61 - 69.
MLA	Khan Mansoor,YILMAZ Erkan,Soylak Mustafa Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. , 2017, ss.61 - 69.
AMA	Khan M,YILMAZ E,Soylak M Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. . 2017; 61 - 69.
Vancouver	Khan M,YILMAZ E,Soylak M Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. . 2017; 61 - 69.
IEEE	Khan M,YILMAZ E,Soylak M "Supramolecular solvent microextraction of uranium at trace levels from water and soil samples." , ss.61 - 69, 2017.
ISNAD	Khan, Mansoor vd. "Supramolecular solvent microextraction of uranium at trace levels from water and soil samples". (2017), 61-69.

APA	Khan M, YILMAZ E, Soylak M (2017). Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. Turkish Journal of Chemistry, 41(1), 61 - 69.
Chicago	Khan Mansoor,YILMAZ Erkan,Soylak Mustafa Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. Turkish Journal of Chemistry 41, no.1 (2017): 61 - 69.
MLA	Khan Mansoor,YILMAZ Erkan,Soylak Mustafa Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. Turkish Journal of Chemistry, vol.41, no.1, 2017, ss.61 - 69.
AMA	Khan M,YILMAZ E,Soylak M Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. Turkish Journal of Chemistry. 2017; 41(1): 61 - 69.
Vancouver	Khan M,YILMAZ E,Soylak M Supramolecular solvent microextraction of uranium at trace levels from water and soil samples. Turkish Journal of Chemistry. 2017; 41(1): 61 - 69.
IEEE	Khan M,YILMAZ E,Soylak M "Supramolecular solvent microextraction of uranium at trace levels from water and soil samples." Turkish Journal of Chemistry, 41, ss.61 - 69, 2017.
ISNAD	Khan, Mansoor vd. "Supramolecular solvent microextraction of uranium at trace levels from water and soil samples". Turkish Journal of Chemistry 41/1 (2017), 61-69.