Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction

KOCUROVA, Livia; ANTOLOVA, Tatiana; BALOGH, Ioseph S.; SANDREJOVA, Jana; BAZEL, Yaroslav; ZARUBA, Serhii; VISHNIKIN, Andriy B.; ANDRUCH, Vasil

Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction

Tatiana ANTOLOVA, (Department of Analytical Chemistry, Pavol Jozef Safarik University, Kosice, Slovaki)

Serhii ZARUBA, (Department of Analytical Chemistry, Faculty of Chemistry, Oles Honchar Dnipropetrovsk National niversity, Dnipropetrovsk, Ukraine)

Jana SANDREJOVA, (Department of Analytical Chemistry, Pavol Jozef Safarik University, Kosice, Slovaki)

Livia KOCUROVA, (Department of Analytical Chemistry, Pavol Jozef Safarik University, Kosice, Slovaki)

Andriy B. VISHNIKIN, (Department of Analytical Chemistry, Faculty of Chemistry, Oles Honchar Dnipropetrovsk National niversity, Dnipropetrovsk, Ukraine)

Yaroslav BAZEL, (Department of Analytical Chemistry, Pavol Jozef Safarik University, Kosice, Slovaki)

Vasil ANDRUCH, (Department of Analytical Chemistry, Pavol Jozef Safarik University, Kosice, Slovaki)

Ioseph S. BALOGH (Department of Chemistry, University of Nyiregyhaza, Nyiregyhaza, Hungary)

Turkish Journal of Chemistry

2 0

Yıl: 2016 Cilt: 40 Sayı: 6 Sayfa Aralığı: 965 - 973 Metin Dili: İngilizce İndeks Tarihi: 29-07-2022

Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction

Öz:

A novel method for the determination of mercury(II) is suggested. The procedure is based on the formationof an ion associate between the bromide complex of Hg(II) and Astrazon Red 6B dye and vortex-assisted liquid{liquidmicroextraction of the ion associate formed, with subsequent spectrophotometric detection. The variables that affectthe procedure, such as pH, the concentration of ligand and dye, the type and volume of extraction solvent, and the rateand time of vortex mixing, were optimized. Under optimum conditions (pH 2.0, 0.01 mol L1KBr, 2 104molL1AR6B, 50 L of the extraction mixture toluene:dichlorethane, 4:1, v:v, vortex mixing for 100 s at 1600 rpm) thelinear range was 8 to 200 g L1Hg(II), with the limit of detection at 1.5 g L1. The method was applied to thedetermination of mercury in water samples.

Anahtar Kelime:

Konular: Mühendislik, Kimya

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	ANTOLOVA T, ZARUBA S, SANDREJOVA J, KOCUROVA L, VISHNIKIN A, BAZEL Y, ANDRUCH V, BALOGH I (2016). Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. , 965 - 973.
Chicago	ANTOLOVA Tatiana,ZARUBA Serhii,SANDREJOVA Jana,KOCUROVA Livia,VISHNIKIN Andriy B.,BAZEL Yaroslav,ANDRUCH Vasil,BALOGH Ioseph S. Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. (2016): 965 - 973.
MLA	ANTOLOVA Tatiana,ZARUBA Serhii,SANDREJOVA Jana,KOCUROVA Livia,VISHNIKIN Andriy B.,BAZEL Yaroslav,ANDRUCH Vasil,BALOGH Ioseph S. Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. , 2016, ss.965 - 973.
AMA	ANTOLOVA T,ZARUBA S,SANDREJOVA J,KOCUROVA L,VISHNIKIN A,BAZEL Y,ANDRUCH V,BALOGH I Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. . 2016; 965 - 973.
Vancouver	ANTOLOVA T,ZARUBA S,SANDREJOVA J,KOCUROVA L,VISHNIKIN A,BAZEL Y,ANDRUCH V,BALOGH I Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. . 2016; 965 - 973.
IEEE	ANTOLOVA T,ZARUBA S,SANDREJOVA J,KOCUROVA L,VISHNIKIN A,BAZEL Y,ANDRUCH V,BALOGH I "Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction." , ss.965 - 973, 2016.
ISNAD	ANTOLOVA, Tatiana vd. "Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction". (2016), 965-973.

APA	ANTOLOVA T, ZARUBA S, SANDREJOVA J, KOCUROVA L, VISHNIKIN A, BAZEL Y, ANDRUCH V, BALOGH I (2016). Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. Turkish Journal of Chemistry, 40(6), 965 - 973.
Chicago	ANTOLOVA Tatiana,ZARUBA Serhii,SANDREJOVA Jana,KOCUROVA Livia,VISHNIKIN Andriy B.,BAZEL Yaroslav,ANDRUCH Vasil,BALOGH Ioseph S. Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. Turkish Journal of Chemistry 40, no.6 (2016): 965 - 973.
MLA	ANTOLOVA Tatiana,ZARUBA Serhii,SANDREJOVA Jana,KOCUROVA Livia,VISHNIKIN Andriy B.,BAZEL Yaroslav,ANDRUCH Vasil,BALOGH Ioseph S. Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. Turkish Journal of Chemistry, vol.40, no.6, 2016, ss.965 - 973.
AMA	ANTOLOVA T,ZARUBA S,SANDREJOVA J,KOCUROVA L,VISHNIKIN A,BAZEL Y,ANDRUCH V,BALOGH I Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. Turkish Journal of Chemistry. 2016; 40(6): 965 - 973.
Vancouver	ANTOLOVA T,ZARUBA S,SANDREJOVA J,KOCUROVA L,VISHNIKIN A,BAZEL Y,ANDRUCH V,BALOGH I Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction. Turkish Journal of Chemistry. 2016; 40(6): 965 - 973.
IEEE	ANTOLOVA T,ZARUBA S,SANDREJOVA J,KOCUROVA L,VISHNIKIN A,BAZEL Y,ANDRUCH V,BALOGH I "Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction." Turkish Journal of Chemistry, 40, ss.965 - 973, 2016.
ISNAD	ANTOLOVA, Tatiana vd. "Spectrophotometric determination of mercury using vortex-assisted liquid{liquidmicroextraction". Turkish Journal of Chemistry 40/6 (2016), 965-973.