Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract
Yıl: 2019 Cilt: 40 Sayı: 1 Sayfa Aralığı: 170 - 172 Metin Dili: İngilizce DOI: 10.17776/csj.455259 İndeks Tarihi: 27-01-2020
Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract
Öz: The synthesis and characterization of Ag nanoparticles from Citrus limonum (lemon leaves)collected the Eastern Black Sea region was investigated in this study. A household microwave system devicewas used for microwave extraction of lemon leaves samples. The extract was prepared by taking 10g of driedlemon leaves. 10 g of sample was shaken in 100 mL of water for 90 min and extracted in a householdmicrowave device at 4 minutes, 600 W. Ag nanoparticles were synthesized that the obtained aqueous solutionwas taken in different volumes by mixing 1 mM and 5mM AgNO3 solution. The colloid solution wassubjected to microwave in an oven 1, 3, 5, 10, 15, 20 and 30 minutes at 90, 180, 360 W. Then production ofAgNPs, the mixture was watched by UV-Vis spectroscopy (Shimadzu UVP-1240 spectrophotometer)measurements at different wavelengths (300 – 800 nm) for SPR of silver nanoparticles. The transition fromyellow to a dark brown, shows the synthesis of silver nanoparticles.
Anahtar Kelime: Limon Yaprakları Ekstraktından Ag Nanopartiküllerin Biyosentezi ve Karakterizasyonu
Öz: Bu çalışmada, Doğu Karadeniz Bölgesinde toplanan limon yapraklarından (Citrus limonum) Ag nanopartiküllerin sentezi ve karakterizasyonu araştırılmıştır. Limon yaprağı örneklerinin mikrodalga ekstraksiyonu için bir ev mikrodalga sistemi cihazı kullanıldı.10 g kurutulmuş limon yaprağı alınarak ekstrakt hazırlandı. Oda sıcaklığında, 10 g numune 100 mL suda 90 dakika çalkalandı ve bir ev mikrodalga cihazında, 600 W gücünde 4 dakika ekstrakte edildi, elde edilen sulu çözeltiden farklı hacimler alınarak 100 mL AgN03(1, 5 mM) çözeltisi ile karıştırılır ve karışım, 90, 180, 360 W gücünde 1, 3, 5, 10, 15, 20 ve 30 dakika boyunca mikrodalgaya maruz bırakılarak Ag nanopartikülleri sentezlendi. Daha sonra üretilen AgNP'lerin kolloid çözeltisi, AgNP'lerin yüzey plazmon rezonansı (SPR) için UV-Vis spektroskopisi ile (Shimadzu UVP- 1240 spektrofotometre) farklı dalga boylarında (300 - 800 nm) ölçümleriyle izlendi. Sarıdan koyu kahverengiye renk değişimi gümüş nanopartiküllerin sentezini gösterir.
Anahtar Kelime: Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık
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| APA | SERDAR G, ALBAY C, SÖKMEN M (2019). Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. , 170 - 172. 10.17776/csj.455259 |
| Chicago | SERDAR GÖNÜL,ALBAY Cansu,SÖKMEN Münevver Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. (2019): 170 - 172. 10.17776/csj.455259 |
| MLA | SERDAR GÖNÜL,ALBAY Cansu,SÖKMEN Münevver Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. , 2019, ss.170 - 172. 10.17776/csj.455259 |
| AMA | SERDAR G,ALBAY C,SÖKMEN M Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. . 2019; 170 - 172. 10.17776/csj.455259 |
| Vancouver | SERDAR G,ALBAY C,SÖKMEN M Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. . 2019; 170 - 172. 10.17776/csj.455259 |
| IEEE | SERDAR G,ALBAY C,SÖKMEN M "Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract." , ss.170 - 172, 2019. 10.17776/csj.455259 |
| ISNAD | SERDAR, GÖNÜL vd. "Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract". (2019), 170-172. https://doi.org/10.17776/csj.455259 |
| APA | SERDAR G, ALBAY C, SÖKMEN M (2019). Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. Cumhuriyet Science Journal, 40(1), 170 - 172. 10.17776/csj.455259 |
| Chicago | SERDAR GÖNÜL,ALBAY Cansu,SÖKMEN Münevver Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. Cumhuriyet Science Journal 40, no.1 (2019): 170 - 172. 10.17776/csj.455259 |
| MLA | SERDAR GÖNÜL,ALBAY Cansu,SÖKMEN Münevver Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. Cumhuriyet Science Journal, vol.40, no.1, 2019, ss.170 - 172. 10.17776/csj.455259 |
| AMA | SERDAR G,ALBAY C,SÖKMEN M Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. Cumhuriyet Science Journal. 2019; 40(1): 170 - 172. 10.17776/csj.455259 |
| Vancouver | SERDAR G,ALBAY C,SÖKMEN M Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract. Cumhuriyet Science Journal. 2019; 40(1): 170 - 172. 10.17776/csj.455259 |
| IEEE | SERDAR G,ALBAY C,SÖKMEN M "Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract." Cumhuriyet Science Journal, 40, ss.170 - 172, 2019. 10.17776/csj.455259 |
| ISNAD | SERDAR, GÖNÜL vd. "Biosynthesis and Characterizatıon of Silver Nanopartıiles from the Lemon Leaves Extract". Cumhuriyet Science Journal 40/1 (2019), 170-172. https://doi.org/10.17776/csj.455259 |
