Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water

YALÇIN, MUSTAFA SERKAN; ozdemir, sadin; Soylak, Mustafa; Kılınç, Ersin

Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water

Sadin ÖZDEMİR, (Mersin Üniversitesi)

Mustafa Serkan YALÇIN, (Mersin Üniversitesi)

Ersin KILINÇ, (Dicle Üniversitesi)

Mustafa SOYLAK (Erciyes Üniversitesi)

Turkish Journal of Chemistry

2 0

Yıl: 2019 Cilt: 43 Sayı: 5 Sayfa Aralığı: 1217 - 1228 Metin Dili: İngilizce İndeks Tarihi: 08-05-2020

Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water

Öz:

A method for preconcentration of Al(III) prior to its determination by inductively coupled plasma-opticalemission spectrometry (ICP-OES) was developed because the sensitivity of ICP-OES is insufficient for trace-level measurement of Al(III). The method is based on the use of Coriolus versicolor-immobilized γ -Fe 2 O3 magnetic nanoparticles as a solid phase sorbent. The best experimental conditions were found as pH 6.0, 2.0 mL/min flow rate, 100 mg amount of C. versicolor on 150 mg of γ -Fe 2 O3 nanoparticles, and 500 mL of sample volume. The Al(III) absorbed on biosorbent was eluted with 5.0 mL of 1.0 mol/L HCl. Limit of detection, limit of quantitation, linear range, correlation coefficient, relative standard deviation, and preconcentration factor were achieved as 0.03 ng/mL, 0.11 ng/mL, 0.2 to 20 ng/mL, 0.9994, 3%, and 100, respectively. Al(III) was preconcentrated in different water and food samples after successful results were achieved in the case of certified reference samples.

Anahtar Kelime:

Konular: Kimya, Analitik Kimya, Uygulamalı Kimya, Organik Kimya, Tıbbi Mühendislik, Kimya Kimya, İnorganik ve Nükleer

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	ozdemir s, YALÇIN M, Kılınç E, Soylak M (2019). Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. , 1217 - 1228.
Chicago	ozdemir sadin,YALÇIN MUSTAFA SERKAN,Kılınç Ersin,Soylak Mustafa Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. (2019): 1217 - 1228.
MLA	ozdemir sadin,YALÇIN MUSTAFA SERKAN,Kılınç Ersin,Soylak Mustafa Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. , 2019, ss.1217 - 1228.
AMA	ozdemir s,YALÇIN M,Kılınç E,Soylak M Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. . 2019; 1217 - 1228.
Vancouver	ozdemir s,YALÇIN M,Kılınç E,Soylak M Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. . 2019; 1217 - 1228.
IEEE	ozdemir s,YALÇIN M,Kılınç E,Soylak M "Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water." , ss.1217 - 1228, 2019.
ISNAD	ozdemir, sadin vd. "Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water". (2019), 1217-1228.

APA	ozdemir s, YALÇIN M, Kılınç E, Soylak M (2019). Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. Turkish Journal of Chemistry, 43(5), 1217 - 1228.
Chicago	ozdemir sadin,YALÇIN MUSTAFA SERKAN,Kılınç Ersin,Soylak Mustafa Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. Turkish Journal of Chemistry 43, no.5 (2019): 1217 - 1228.
MLA	ozdemir sadin,YALÇIN MUSTAFA SERKAN,Kılınç Ersin,Soylak Mustafa Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. Turkish Journal of Chemistry, vol.43, no.5, 2019, ss.1217 - 1228.
AMA	ozdemir s,YALÇIN M,Kılınç E,Soylak M Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. Turkish Journal of Chemistry. 2019; 43(5): 1217 - 1228.
Vancouver	ozdemir s,YALÇIN M,Kılınç E,Soylak M Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water. Turkish Journal of Chemistry. 2019; 43(5): 1217 - 1228.
IEEE	ozdemir s,YALÇIN M,Kılınç E,Soylak M "Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water." Turkish Journal of Chemistry, 43, ss.1217 - 1228, 2019.
ISNAD	ozdemir, sadin vd. "Magnetic solid-phase extraction based on Coriolus versicolor-immobilized γ -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water". Turkish Journal of Chemistry 43/5 (2019), 1217-1228.