The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material

Koyuncu, Dilsad Dolunay Eslek

doi:10.16984/saufenbilder.755286

The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material

Dilşad Dolunay ESLEK KOYUNCU (Gazi Üniversitesi, Ankara, Türkiye)

Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi

7 0

Yıl: 2021 Cilt: 25 Sayı: 1 Sayfa Aralığı: 240 - 251 Metin Dili: İngilizce DOI: 10.16984/saufenbilder.755286 İndeks Tarihi: 11-06-2021

The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material

Öz:

The combined effect of hydrothermal treatment temperature and aging time on the structuralproperties of ordered mesoporous KIT-6 material were investigated. A series of KIT-6 materialswere prepared by hydrothermal synthesis procedure. In the first step, experiments wereperformed at 90oC and at different aging times (0-72 h) to understand the effect of hydrothermalaging time. It was concluded that the aging time positively affect the formation of orderedmesoporous structure and uniform pore structure occurs after 18 h. In addition, longhydrothermal treatment time favored the pore enlargement. In the second step, to understandwhich parameter (time or temperature) is more important in the synthesis of highly uniformmaterial, KIT-6 materials were prepared at different temperatures ranging between 60-150oCand at different aging times (24 h and 72 h). The experiments showed that at elevatedtemperatures (>90oC) long aging times negatively affect the structural properties of themesoporous KIT-6 structure. Highly uniform mesoporous KIT-6 material having highcrystallinity, narrow pore size distribution, high BET surface area (726 cm3/g) and high porevolume (1.5 cm3/g) was prepared at 120oC with an aging time of 24 h. However, it wasdetermined that 60oC is not a suitable temperature to obtain KIT-6 material having goodstructural properties and the uniform crystal structure deteriorated at 150oC.

Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	Koyuncu D (2021). The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. , 240 - 251. 10.16984/saufenbilder.755286
Chicago	Koyuncu Dilsad Dolunay Eslek The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. (2021): 240 - 251. 10.16984/saufenbilder.755286
MLA	Koyuncu Dilsad Dolunay Eslek The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. , 2021, ss.240 - 251. 10.16984/saufenbilder.755286
AMA	Koyuncu D The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. . 2021; 240 - 251. 10.16984/saufenbilder.755286
Vancouver	Koyuncu D The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. . 2021; 240 - 251. 10.16984/saufenbilder.755286
IEEE	Koyuncu D "The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material." , ss.240 - 251, 2021. 10.16984/saufenbilder.755286
ISNAD	Koyuncu, Dilsad Dolunay Eslek. "The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material". (2021), 240-251. https://doi.org/10.16984/saufenbilder.755286

APA	Koyuncu D (2021). The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 25(1), 240 - 251. 10.16984/saufenbilder.755286
Chicago	Koyuncu Dilsad Dolunay Eslek The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi 25, no.1 (2021): 240 - 251. 10.16984/saufenbilder.755286
MLA	Koyuncu Dilsad Dolunay Eslek The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi, vol.25, no.1, 2021, ss.240 - 251. 10.16984/saufenbilder.755286
AMA	Koyuncu D The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi. 2021; 25(1): 240 - 251. 10.16984/saufenbilder.755286
Vancouver	Koyuncu D The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material. Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi. 2021; 25(1): 240 - 251. 10.16984/saufenbilder.755286
IEEE	Koyuncu D "The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material." Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 25, ss.240 - 251, 2021. 10.16984/saufenbilder.755286
ISNAD	Koyuncu, Dilsad Dolunay Eslek. "The Effect of Hydrothermal Aging Time and Temperature on the Structural Properties of KIT-6 Material". Sakarya Üniversitesi Fen Bilimleri Enstitüsü Dergisi 25/1 (2021), 240-251. https://doi.org/10.16984/saufenbilder.755286