Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2

Mustafa Şengör (Marmara Üniversitesi, Teknoloji Fakültesi, Metalürji ve Malzeme Mühendisliği Bölümü, İstanbul, Türkiye)
International journal of advances in engineering and pure sciences (Online)
1 0
Yıl: 2021 Cilt: 33 Sayı: 1 Sayfa Aralığı: 116 - 121 Metin Dili: İngilizce DOI: 10.7240/jeps.771433 İndeks Tarihi: 20-10-2021

Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2

Öz:
Composites of calcinated bovine bone derived hydroxyapatite (BHA) doped 1 and 2 wt% MgF2 were prepared by a sintering process. Microstructure and crystallographic analyses along with measurements of density, compression strength, and microhardness were carried out in the produced samples. The experimental results indicated a beneficial effect of MgF2 in the matrix of BHA reflected in the significant increase of compression strength and microhardness up to 143 MPa and 313 HV, respectively, achieved after sintering at 1300 0C for 2% MgF2 addition. The presence of MgF2 reduced the onset of sintering towards lower temperatures (i.e. 1100 0C) and increased the stability of hydroxyapatite towards transformation to TCP at 1300 0C. The influence of Mg2+ and Fions in the lattice of hydroxyapatite is discussed.
Anahtar Kelime:

MgF2 ile Güçlendirilmiş Sığır Kaynaklı Hidroksiapatit (BHA) Kompozitlerinin Mikroyapısı ve Mekanik Özellikleri

Öz:
Kalsine edilmiş sığır kemiğinden elde edilen hidroksiapatit (BHA) ile ağırlıkça% 1 ve ağırlıkça% 2 MgF2 katkılı kompozitleribir sinterleme işlemi ile hazırlandı. Üretilen numunelerde mikroyapı ve kristalografik analizler ile birlikte yoğunluk, basmamukavemeti ve mikrosertlik ölçümleri yapıldı. Deneysel sonuçlar, % 2 MgF2 ilavesi ve 1300oC'de sinterlemeden sonra eldeedilen BHA matrisin, sıkıştırma mukavemeti ve mikro sertlikteki önemli artışa (sırasıyla 143 MPa ve 313 HV'ye kadar) nedenolduğunu gösterdi. MgF2'nin varlığı, sinterleme başlangıcını daha düşük sıcaklıklara (~ 1100oC) düşürdü ve hidroksiapatitin1300oC'de TCP'ye dönüşüme karşı stabilitesini arttırdı. Mg2 + ve Fiyonlarının hidroksiapatit örgüsündeki etkisi tartışıldı.
Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık
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APA Sengor M (2021). Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. , 116 - 121. 10.7240/jeps.771433
Chicago Sengor Mustafa Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. (2021): 116 - 121. 10.7240/jeps.771433
MLA Sengor Mustafa Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. , 2021, ss.116 - 121. 10.7240/jeps.771433
AMA Sengor M Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. . 2021; 116 - 121. 10.7240/jeps.771433
Vancouver Sengor M Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. . 2021; 116 - 121. 10.7240/jeps.771433
IEEE Sengor M "Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2." , ss.116 - 121, 2021. 10.7240/jeps.771433
ISNAD Sengor, Mustafa. "Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2". (2021), 116-121. https://doi.org/10.7240/jeps.771433
APA Sengor M (2021). Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. International journal of advances in engineering and pure sciences (Online), 33(1), 116 - 121. 10.7240/jeps.771433
Chicago Sengor Mustafa Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. International journal of advances in engineering and pure sciences (Online) 33, no.1 (2021): 116 - 121. 10.7240/jeps.771433
MLA Sengor Mustafa Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. International journal of advances in engineering and pure sciences (Online), vol.33, no.1, 2021, ss.116 - 121. 10.7240/jeps.771433
AMA Sengor M Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. International journal of advances in engineering and pure sciences (Online). 2021; 33(1): 116 - 121. 10.7240/jeps.771433
Vancouver Sengor M Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2. International journal of advances in engineering and pure sciences (Online). 2021; 33(1): 116 - 121. 10.7240/jeps.771433
IEEE Sengor M "Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2." International journal of advances in engineering and pure sciences (Online), 33, ss.116 - 121, 2021. 10.7240/jeps.771433
ISNAD Sengor, Mustafa. "Microstructure and Mechanical Properties of Composites of BovineDerived Hydroxyapatite (BHA) Reinforced with MgF2". International journal of advances in engineering and pure sciences (Online) 33/1 (2021), 116-121. https://doi.org/10.7240/jeps.771433
Sayfa Oluşturulma Tarihi
23-04-2024 19:47

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