Preparation and characterization of templated porous carbons from sucrose by one-pot
method and application as a $CO_2$ adsorbent

Gürbüz, Meltem; TÜMSEK, FATMA

doi:10.3906/kim-2012-11

Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent

Meltem GÜRBÜZ, (Eskişehir Osmangazi Üniversitesi, Mühendislik Mimarlık Fakültesi, Kimya Mühendisliği Bölümü, Eskişehir, Türkiye)

Fatma TÜMSEK (Eskişehir Osmangazi Üniversitesi, Mühendislik Mimarlık Fakültesi, Kimya Mühendisliği Bölümü, Eskişehir, Türkiye)

Turkish Journal of Chemistry

2 0

Yıl: 2021 Cilt: 45 Sayı: 4 Sayfa Aralığı: 1257 - 1269 Metin Dili: İngilizce DOI: 10.3906/kim-2012-11 İndeks Tarihi: 29-06-2022

Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent

Öz:

The templated porous carbons were prepared from sucrose by one-pot method. In this method in which the pre-synthesis of the hard template is eliminated, the porous carbons were produced by organic-inorganic self-assembly of sucrose, tetraethyl ortosilicate (TEOS), Pluronic P123 and n-butanol in an acidic medium, and subsequent carbonization. The synthesis parameters such as sucrose amount, TEOS molar ratio and carbonization temperature were evaluated for describing their effects on the pore structures of the synthesized carbons. The prepared porous carbons were characterized by $N_2$adsorption, thermogravimetric analysis (TGA), Raman spectroscopy, X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), and transmission electron microscopy (TEM) techniques. The carbon dioxide adsorption uptakes of the obtained porous carbons were determined at 1 bar and 273 K. The templated carbon obtained with the lowest TEOS molar ratio exhibited the highest BET surface area of $1289 m^2 /g$ and micropore volume of $0.467 cm^3 /g$, and showed the highest $CO_2$ uptake of 2.28 mmol/g.

Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	Gürbüz M, TÜMSEK F (2021). Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. , 1257 - 1269. 10.3906/kim-2012-11
Chicago	Gürbüz Meltem,TÜMSEK FATMA Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. (2021): 1257 - 1269. 10.3906/kim-2012-11
MLA	Gürbüz Meltem,TÜMSEK FATMA Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. , 2021, ss.1257 - 1269. 10.3906/kim-2012-11
AMA	Gürbüz M,TÜMSEK F Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. . 2021; 1257 - 1269. 10.3906/kim-2012-11
Vancouver	Gürbüz M,TÜMSEK F Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. . 2021; 1257 - 1269. 10.3906/kim-2012-11
IEEE	Gürbüz M,TÜMSEK F "Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent." , ss.1257 - 1269, 2021. 10.3906/kim-2012-11
ISNAD	Gürbüz, Meltem - TÜMSEK, FATMA. "Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent". (2021), 1257-1269. https://doi.org/10.3906/kim-2012-11

APA	Gürbüz M, TÜMSEK F (2021). Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. Turkish Journal of Chemistry, 45(4), 1257 - 1269. 10.3906/kim-2012-11
Chicago	Gürbüz Meltem,TÜMSEK FATMA Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. Turkish Journal of Chemistry 45, no.4 (2021): 1257 - 1269. 10.3906/kim-2012-11
MLA	Gürbüz Meltem,TÜMSEK FATMA Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. Turkish Journal of Chemistry, vol.45, no.4, 2021, ss.1257 - 1269. 10.3906/kim-2012-11
AMA	Gürbüz M,TÜMSEK F Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. Turkish Journal of Chemistry. 2021; 45(4): 1257 - 1269. 10.3906/kim-2012-11
Vancouver	Gürbüz M,TÜMSEK F Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent. Turkish Journal of Chemistry. 2021; 45(4): 1257 - 1269. 10.3906/kim-2012-11
IEEE	Gürbüz M,TÜMSEK F "Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent." Turkish Journal of Chemistry, 45, ss.1257 - 1269, 2021. 10.3906/kim-2012-11
ISNAD	Gürbüz, Meltem - TÜMSEK, FATMA. "Preparation and characterization of templated porous carbons from sucrose by one-pot method and application as a $CO_2$ adsorbent". Turkish Journal of Chemistry 45/4 (2021), 1257-1269. https://doi.org/10.3906/kim-2012-11