Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles
that synthesized with Celosia Cristata flower extract

ÜSTÜN ÖZGÜR, MAHMURE; YAPAÖZ, melda; Duygulu, Ozgur

doi:10.3906/kim-2007-10

Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract

Mahmure ÜSTÜN ÖZGÜR, (Yıldız Teknik Üniversitesi, Fen Edebiyat Fakültesi, Kimya Bölümü, İstanbul, Türkiye)

Özgür DUYGULU, (TÜBİTAK MAM Malzeme Enstitüsü, Kocaeli, Türkiye)

Melda ALTIKATOĞLU YAPAÖZ (Yıldız Teknik Üniversitesi, Fen Edebiyat Fakültesi, Kimya Bölümü, İstanbul, Türkiye)

Turkish Journal of Chemistry

7 0

Yıl: 2022 Cilt: 46 Sayı: 1 Sayfa Aralığı: 59 - 85 Metin Dili: İngilizce DOI: 10.3906/kim-2007-10 İndeks Tarihi: 04-07-2022

Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract

Öz:

Increasing interest in green chemistry has led scientists to an environmentally friendly nanoparticle synthesis approach that has many advantages, such as simple, affordable and versatility for a wide range of commercial production. In this study, green synthesis of zinc oxide nanoparticles (ZnO NPs), which is widely researched in the field of nanotechnology, was performed under different conditions (volume ratio of CC flower extract to $Zn(CH_3 COO)_2$ solution, time, pH and temperature) using the aqueous extract of Amarant (Celosia cristata L., CC, cockscome) plant flowers. Produced ZnO NPs were characterized by UV-Vis absorption spectroscopy, Fourier transform infrared spectroscopy (FTIR), high-resolution transmission electron microscopy (HR-TEM) and scanning electron microscopy (SEM) analysis. The characteristic absorption peak seen at $λ_{max}: 364$ nm in the UV-Vis absorption spectrum and the band seen at $381 cm^{–1}$ in the FTIR spectrum indicate that ZnO NPs were synthesized. TEM image also confirmed the formation of nanoparticles. The average size of nanoparticles is approximately 22–27 nm and the shape of the ZnO NPs as nearly spherical. The effect of different calcination temperatures (100, 200, 300, 400, and 500 °C) on the size of ZnO NPs was investigated and it was observed that the particle size decreased as the calcination temperature increased. ZnO NPs were also used as photo catalyst for removal of basic yellow28 (BY28) and basic violet39 (BV39) dyestuffs which are used in textile industry and ecologically toxic. The decolorization efficiency was found 95%–100% and 62% respectively when the BV39 and BY28 dyestuffs were exposed to UV light for 160 min. Antibacterial activity of ZnO NPs produced with different amounts of CC flower extract and calcined at different temperatures (100, 200, 300, 400, and 500 °C) was investigated using modified disc diffusion method. Produced ZnO NPs displayed antibacterial activity against Staphylococcus aureus and Escherichia coli bacterial strains and were more effective against gram-positive pathogens. The findings displayed that the antibacterial activity of ZnO NPs is related to the particle size.This new environmentally friendly synthesis approach is a suitable technique for large-scale commercial production and can be considered as an alternative to chemical methods.

Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	ÜSTÜN ÖZGÜR M, Duygulu O, YAPAÖZ m (2022). Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. , 59 - 85. 10.3906/kim-2007-10
Chicago	ÜSTÜN ÖZGÜR MAHMURE,Duygulu Ozgur,YAPAÖZ melda Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. (2022): 59 - 85. 10.3906/kim-2007-10
MLA	ÜSTÜN ÖZGÜR MAHMURE,Duygulu Ozgur,YAPAÖZ melda Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. , 2022, ss.59 - 85. 10.3906/kim-2007-10
AMA	ÜSTÜN ÖZGÜR M,Duygulu O,YAPAÖZ m Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. . 2022; 59 - 85. 10.3906/kim-2007-10
Vancouver	ÜSTÜN ÖZGÜR M,Duygulu O,YAPAÖZ m Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. . 2022; 59 - 85. 10.3906/kim-2007-10
IEEE	ÜSTÜN ÖZGÜR M,Duygulu O,YAPAÖZ m "Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract." , ss.59 - 85, 2022. 10.3906/kim-2007-10
ISNAD	ÜSTÜN ÖZGÜR, MAHMURE vd. "Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract". (2022), 59-85. https://doi.org/10.3906/kim-2007-10

APA	ÜSTÜN ÖZGÜR M, Duygulu O, YAPAÖZ m (2022). Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. Turkish Journal of Chemistry, 46(1), 59 - 85. 10.3906/kim-2007-10
Chicago	ÜSTÜN ÖZGÜR MAHMURE,Duygulu Ozgur,YAPAÖZ melda Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. Turkish Journal of Chemistry 46, no.1 (2022): 59 - 85. 10.3906/kim-2007-10
MLA	ÜSTÜN ÖZGÜR MAHMURE,Duygulu Ozgur,YAPAÖZ melda Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. Turkish Journal of Chemistry, vol.46, no.1, 2022, ss.59 - 85. 10.3906/kim-2007-10
AMA	ÜSTÜN ÖZGÜR M,Duygulu O,YAPAÖZ m Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. Turkish Journal of Chemistry. 2022; 46(1): 59 - 85. 10.3906/kim-2007-10
Vancouver	ÜSTÜN ÖZGÜR M,Duygulu O,YAPAÖZ m Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract. Turkish Journal of Chemistry. 2022; 46(1): 59 - 85. 10.3906/kim-2007-10
IEEE	ÜSTÜN ÖZGÜR M,Duygulu O,YAPAÖZ m "Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract." Turkish Journal of Chemistry, 46, ss.59 - 85, 2022. 10.3906/kim-2007-10
ISNAD	ÜSTÜN ÖZGÜR, MAHMURE vd. "Investigation of antibacterial and photocatalytic efficiency of green ZnO nanoparticles that synthesized with Celosia Cristata flower extract". Turkish Journal of Chemistry 46/1 (2022), 59-85. https://doi.org/10.3906/kim-2007-10