Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi

Özlem ALTINTAŞ YILDIRIM (KONYA TEKNİK ÜNİVERSİTESİ, MÜHENDİSLİK VE DOĞA BİLİMLERİ FAKÜLTESİ, METALURJİ VE MALZEME MÜHENDİSLİĞİ BÖLÜMÜ)
İsa GÖKÇE, (KONYA TEKNİK ÜNİVERSİTESİ, MÜHENDİSLİK VE DOĞA BİLİMLERİ FAKÜLTESİ, METALURJİ VE MALZEME MÜHENDİSLİĞİ BÖLÜMÜ)
Hüsnü Emrah ÜNALAN (KONYA TEKNİK ÜNİVERSİTESİ, MÜHENDİSLİK VE DOĞA BİLİMLERİ FAKÜLTESİ, METALURJİ VE MALZEME MÜHENDİSLİĞİ BÖLÜMÜ)
Mehmet Can YILDIRIM, (KONYA TEKNİK ÜNİVERSİTESİ, MÜHENDİSLİK VE DOĞA BİLİMLERİ FAKÜLTESİ, METALURJİ VE MALZEME MÜHENDİSLİĞİ BÖLÜMÜ)
Savaş SÖNMEZOĞLU, (KONYA TEKNİK ÜNİVERSİTESİ, MÜHENDİSLİK VE DOĞA BİLİMLERİ FAKÜLTESİ, METALURJİ VE MALZEME MÜHENDİSLİĞİ BÖLÜMÜ)
Teoman ÖZTÜRK (KONYA TEKNİK ÜNİVERSİTESİ, MÜHENDİSLİK VE DOĞA BİLİMLERİ FAKÜLTESİ, METALURJİ VE MALZEME MÜHENDİSLİĞİ BÖLÜMÜ)
9 4

Proje Grubu: MAG Sayfa Sayısı: 194 Proje No: 216M011 Proje Bitiş Tarihi: 01.12.2019 Metin Dili: Türkçe İndeks Tarihi: 29-03-2021

Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi

Öz:
Gerçeklestirilen projenin genel amacı, antibakteriyel malzeme üretim süreçleri üzerinde yogunlasan, yapısal ve fonksiyonel özellikler kazandırılmıs ileri malzemelerin gelistirilmesidir. Bu genel amaç kapsamında yapılan çalısmalarda yeni nesil çinko kalay oksit (ZTO) ile metal asılanmıs indirgenmis grafen oksittin (rGO-M, M=Mn-Co) olusturdugu kompozitler (ZTO-rGOM) sentezlenmistir. Kompozitlerin hastane ortamında bulunan bakterilere karsı gösterecekleri antibakteriyel özellikle dogru orantılı olan fotokatalitik aktivitelerindeki degisimler detaylı bir sekilde incelenmistir. Son olarak en iyi fotokatalitik aktivite gösteren kompozit kompozisyonlarının antibakteriyel aktivite testleri gerçeklestirilmistir. Yapılan çalısmalar üç asamada gerçeklestirilmistir; ?Projenin ilk bölümünde modifiye edilmis Hummers yöntemi ile oksitlenmis grafitin bilyeli ögütme islemiyle kısmi indirgenmesi sonucunda grafen oksit (GO) elde edilmistir. GO kimyasal indirgenme reaksiyonuna maruz bırakılıp tamamıyla indirgenmesi saglanarak rGO sentezlenmistir. Son olarak rGO yapısına düsük oranlarda (% 0, 0.2, 0.4, 0.6, 0.8 ve 1.0) Co ve Mn metal ilavesi yapılarak rGO?M?lerin üretimi gerçeklestirilmistir ?Projenin ikinci bölümü ise ZTO nano yapıların hidrotermal yöntem kullanılarak sentezlenmesini kapsamaktadır. Yüksek kristallige sahip ZTO nano yapılar kontrollü ve tekrarlanabilir bir yöntem olan hidrotermal yöntemle sentezlenebilmesi için gerekli optimum deneysel sartlar sistematik bir deney çalısması ile belirlenmistir. Sentezlenen ZTO nano yapılara sentez sıcaklıgı, süresi, baslangıç kimyasallarının konsantrasyon oranı, çözelti pH?ı ve çözücü ortamı gibi deneysel parametrelerin etkisi incelenmistir. ?Optimum sentez sartlarında üretilen ZTO nanoparçacıkların hem UV ve hem de görünür ısık altında Rodamin B (RhB) boyasına karsı fotokatalitik aktiviteleri detaylı bir sekilde incelenmistir. Aktivite tayinlerinde ZTO nanoparçacıkların UV ısık altında 120 dakikada RhB boyasının %97.9?unu bozarken görünür ısıkda 400 dakikada boyanın %88.2?sini bozdugu gözlemlenmistir. Bu sonuçların ZTO nanoparçacıkların fotokatalitik aktivitelerini inceleyen literatürdeki çalısmalarla kıyaslandıgı zaman oldukça iyi sonuçlar oldugu görülmektedir. ?Projenin son bölümü ise uygulamaya yönelik olup önceki iki bölümde belirlenen optimum özelliklere sahip rGO-M ve ZTO nano yapılar ile ZTO-rGO-M kompozitlerin hidrotermal yöntemle üretilmesini içermektedir. Bu bölümde ayrıca ZTO-rGO-M kompozitlerin fotokatalitik aktivitelerinin belirlenmesi ve optimum fotokatalitik aktivite gösteren kompozit kompozisyonunun S. aureus ve E. coli bakterilerine karsı aktivitelerini belirlemek amacıyla antibakteriyel testlerinin yapılmasını kapsamaktadır. ZTO?rGO yapılarının fotokatalitik aktiviteleri incelendiginde ise ZTO?rGO?nun fotokatalitik aktivitesinin saf ZTO?ya kıyasla oldukça iyilestigi ve metal asılamanın fotokatalitik aktiviteyi optimum asılama miktarına (%1.0) kadar arttırıcı özellik gösterdigi gözlemlenmistir. ? Projenin genel amacı dogrultusunda kompozit yapıların antibakteriyel testleri disk difüzyon yöntemi ile gerçeklestirilmistir. Çalısmalar sonucunda optimum antibakteriyel özellik saglayan kompozisyonun 25 mg kompozit/mL konsantrasyonunda hazırlanan %1.0 Mn asılanmıs ZTO?rGO?Mn oldugu belirlenmistir. Antibakteriyel testlerden elde edilen sonuçlara göre ZTO?rGO-M kompozit yapıların ZTO?rGO kompozitlerle kıyaslandıgında bakterilere karsı daha aktif özellik sergilese de genel olarak zayıf bir antibakteriyel aktivite gösterdigi belirlenmistir. Bu durumun disk difüzyon yönteminin suda çözünen malzemelere daha uygun olmasından kaynaklandıgı düsünülmektedir. Antibakteriyel özelliklerin daha dogru belirlenebilmesi için uygulanan disk difüzyon yöntemi yerine; kompozitlerin ve bakterilerin solüsyon içerisinde dagıtıldıktan belirli bir süre sonra solüsyonda kalan bakteri sayısının sayılması esasına dayanan çözelti-bazlı bir yöntemle antibakteriyel özelliklerin belirlenmesi planlanmaktadır
Anahtar Kelime: antibakteriyel özellik fotokatalitik aktivite rgo-zto kompozit hidrotermal yöntem zto

Konular: Metalürji Mühendisliği
Erişim Türü: Erişime Açık
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APA YILDIRIM Ö, GOKCE I, YILDIRIM M, ÜNALAN H, SÖNMEZOĞLU S, Ozturk T (2019). Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. , 1 - 194.
Chicago YILDIRIM Özlem ALTINTAŞ,GOKCE Isa,YILDIRIM Mehmet Can,ÜNALAN Hüsnü Emrah,SÖNMEZOĞLU Savaş,Ozturk Teoman Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. (2019): 1 - 194.
MLA YILDIRIM Özlem ALTINTAŞ,GOKCE Isa,YILDIRIM Mehmet Can,ÜNALAN Hüsnü Emrah,SÖNMEZOĞLU Savaş,Ozturk Teoman Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. , 2019, ss.1 - 194.
AMA YILDIRIM Ö,GOKCE I,YILDIRIM M,ÜNALAN H,SÖNMEZOĞLU S,Ozturk T Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. . 2019; 1 - 194.
Vancouver YILDIRIM Ö,GOKCE I,YILDIRIM M,ÜNALAN H,SÖNMEZOĞLU S,Ozturk T Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. . 2019; 1 - 194.
IEEE YILDIRIM Ö,GOKCE I,YILDIRIM M,ÜNALAN H,SÖNMEZOĞLU S,Ozturk T "Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi." , ss.1 - 194, 2019.
ISNAD YILDIRIM, Özlem ALTINTAŞ vd. "Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi". (2019), 1-194.
APA YILDIRIM Ö, GOKCE I, YILDIRIM M, ÜNALAN H, SÖNMEZOĞLU S, Ozturk T (2019). Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. , 1 - 194.
Chicago YILDIRIM Özlem ALTINTAŞ,GOKCE Isa,YILDIRIM Mehmet Can,ÜNALAN Hüsnü Emrah,SÖNMEZOĞLU Savaş,Ozturk Teoman Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. (2019): 1 - 194.
MLA YILDIRIM Özlem ALTINTAŞ,GOKCE Isa,YILDIRIM Mehmet Can,ÜNALAN Hüsnü Emrah,SÖNMEZOĞLU Savaş,Ozturk Teoman Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. , 2019, ss.1 - 194.
AMA YILDIRIM Ö,GOKCE I,YILDIRIM M,ÜNALAN H,SÖNMEZOĞLU S,Ozturk T Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. . 2019; 1 - 194.
Vancouver YILDIRIM Ö,GOKCE I,YILDIRIM M,ÜNALAN H,SÖNMEZOĞLU S,Ozturk T Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi. . 2019; 1 - 194.
IEEE YILDIRIM Ö,GOKCE I,YILDIRIM M,ÜNALAN H,SÖNMEZOĞLU S,Ozturk T "Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi." , ss.1 - 194, 2019.
ISNAD YILDIRIM, Özlem ALTINTAŞ vd. "Yeni nesil Zn2SnO4–GO–M (M: Mn, Co) foto katalizör kompozit yapıların sentezi, karakterizasyonu ve antibakteriyel özelliklerinin incelenmesi". (2019), 1-194.
Sayfa Oluşturulma Tarihi
24-04-2024 1:47

İLETİŞİM

TÜBİTAK ULAKBİM TR Dizin

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